Determination of Ceftazidime by Flow Injection Chemiluminescence
  
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DOI:10.3969/j.issn.1004-4957.年份.月份
KeyWord:chemiluminescence  flow injection analysis  luminol  ceftazidime  gold nano particle
  
AuthorInstitution
WANG Jue,QU Jianying,ZHU Lili,WANG Jinzhong,WANG Yue 河南大学化学化工学院环境与分析科学研究所
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Abstract:
      In alkaline medium,gold nano particle could catalyze the chemiluminescence(CL)of the luminol-potassium permanganate system,and the presence of ceftazidime could enhance the CL intensity of this system.Based on this,a flow injection CL method for the determination of ceftazidime was established.Under the optimized conditions,the linear range for determination of ceftazidime was in the range of 30×10-5-50×10-2 g/L with a detection limit of 10×10-5 g/L.The relative standard deviation(RSD,n=11) was 20% for 40×10-3 g/L ceftazidime.The method was applied in the determination of ceftazidime in injection with satisfactory results.
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