|
| Study on Specific Chromatogram of Ginger Essential Oil by Ultra Performance Convergence Chromatography |
| |
| View Full Text Download reader |
| DOI： |
| KeyWord:ginger essential oil ultra performance convergence chromatography（UPC2） specific chromatogram |
| Author | Institution |
| SONG Wei,HAN Fang,DING Lei,ZHOU Dian-bing,JIA Xue-ying,LV Ya-ning,DENG Xiao-jun,ZHENG Ping,SHENG Xuan,HU Yan-yun |
1.Technical Center for Inspection and Quarantine of Anhui Entry-Exit Inspection and Quarantine Bureau;2.Anhui Province Key Laboratory of Analysis and Detection for Food Safety;3.Shanghai Academy of Science and Technology for Inspection and Quarantine |
|
| Hits: 2503 |
| Download times: 1057 |
| Abstract: |
| Specific chromatogram of ginger essential oil was studied by ultra performance convergence chromatographic(UPC2) method.The ginger essential oil was diluted with n heptane,and separated on UPC2 system with photo diode array(PDA) detector,using supercritical CO2 as mobile phase and acetonitrile as cosolvent at a flow rate of 08 mL/min by gradient elution.A spectral library for characteristic peaks and standard specific chromatogram of ginger essential oil from Anhui was established.By comparison with the characteristic peaks from PDA library and similarity evaluation,the resemblance of specific chromatogram was found higher than 09 among the ginger essential oil from Anhui and the standard control.The relative standard deviations(RSD) for relative retention time and relative peak area of common peaks were less than 30%.This method has good precision,reproducibility and stability,and could meet the requirements for the evaluation of specific chromatogram.Coupled with cluster analysis and principal component analysis,the UPC2 specific chromatogram method was successfully used to distinguish 20 samples from different habitats.This study provided a novel,convenient and rapid method for the quality control and origin traceability of ginger essential oil. |
| Close |
|
|
|